HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 59925880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 59180449 | HCID 59180449 | — |
| Reactant | HCID 86638763 | HCID 86638763 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 59925880 | HCID 59925880 | — |
Reaction Steps
Synthesized as described for 2 using a 3:1 regioisomeric mixture of 107 (23.68 g; 0.10 mol) and 2-tert-butyl-4-fluorobenzenesulfonic acid, phosphorus pentachloride (23.13 g; 0.11 mol) and dichloroethane (700 mL). The title compound was obtained as a white solid which was a 1:1 regioisomeric ratio of itself and 2-tert-butyl-4-fluorobenzene-1-sulfonyl chloride (10.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178699B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-e9c3485f2f764b52b48fc9d00d11dd23 |
| Source note | uspto-grants-2012_05 |