HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-(3-fluorobenzyloxy)aniline → HCID 57597277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-(3-fluorobenzyloxy)aniline | HCID 7059263 | — |
| Reactant | 4-Chloro-5-ethyl-5H-pyrrolo[3,2-d]pyrimidine | HCID 71413460 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 57597277 | HCID 57597277 | 52.8% |
Reaction Steps
To a solution of 4-chloro-5-ethyl-5H-pyrrolo[3,2-d]pyrimidine (85 mg) in 1-methyl-2-pyrrolidone (0.94 mL) was added 3-chloro-4-[(3-fluorobenzyl)oxy]aniline (177 mg). The title compound (98 mg) was obtained as a pale-purple powder crystals by the reaction in the same manner as in Example 29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178543B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-9f223d7b534044d5832cc77e42c3e4b1 |
| Source note | uspto-grants-2012_05 |