HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-Bromobenzyl)-2,2-dimethoxyacetamide → HCID 178515305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-Bromobenzyl)-2,2-dimethoxyacetamide | HCID 67520671 | — |
| Reactant | HCID 178515296 | HCID 178515296 | — |
| Reactant | HCID 178515312 | HCID 178515312 | — |
| Product | HCID 178515305 | HCID 178515305 | — |
Reaction Steps
The title compounds was obtained as a yellow solid following the procedure for 5-bromoisoquinolin-3-ol and 7-bromoisoquinolin-3-ol, using N-(4-bromobenzyl)-2,2-dimethoxyacetamide. 1H NMR (400 MHz, DMSO-d6): δ=6.87 (s, 1H), 7.42 (dd, J=2.0 & 8.4 Hz, 1H), 7.87 (d, J=8.8 Hz, 1H), 8.00 (d, J=2.0 Hz, 1H), 8.93 (s, 1H), 11.07 (brs, 1H). MS(ES+): m/z=224.04/225.93 (88/100) [MH+]. HPLC: tR=2.41 min (polar—5 min, ZQ3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178668B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-730aabb5b2c444969acda76fc5bda047 |
| Source note | uspto-grants-2012_05 |