HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1926294Generated: November 1, 2026
4-Chlorobenzylamine → HCID 67521395, compound
https://huagongshe.com/reaction/1926294
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chlorobenzylamine | HCID 66036 | — |
| Reactant | Acetic acid, 2,2-dimethoxy-, methyl ester | HCID 66647 | — |
| Product | HCID 67521395 | HCID 67521395 | — |
Reaction Steps
Into a vial was added methyl dimethoxyacetate (0.98 g, 7.3 mmol) and 4-chlorobenzylamine (1.0 g, 7.3 mmol), this mixture was stirred at 50° C. for 2 d. The product was recrystallized from Heptane to yield the desired product as an oil that solidified over time. MS (ES+): m/z=244.09/246.05 [MH+]. HPLC: tR=2.80 min (ZQ2, polar—5 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08178668B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-cd8ccc7957af4ffb874569d854c7f9c6 |
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| Source note | uspto-grants-2012_05 |
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