HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1926398Generated: November 2, 2026
2-Bromo-3-methoxyaniline → 2-Chloro-7-methoxy-1,3-benzothiazole
https://huagongshe.com/reaction/1926398
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Bromo-3-methoxyaniline | HCID 10910575 | — |
| Reactant | 2,5-Dichloro-1,3-benzothiazole | HCID 13314816 | — |
| Reactant | HCID 178489024 | HCID 178489024 | — |
| Product | 2-Chloro-7-methoxy-1,3-benzothiazole | HCID 55276589 | — |
Reaction Steps
The title compound was prepared from 2-bromo-3-methoxyaniline via 2-mercapto-7-methoxy-1,3-benzothiazole as described for 2,5-dichloro-1,3-benzothiazole except that in the first step the reaction mixture was heated to 120° C. for 10 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08178668B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-d3481608d2774da4a86698670aa7a252 |
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| Source note | uspto-grants-2012_05 |
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