HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Difluoroaniline → 2-Iodo-5-methylbenzo[d]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Difluoroaniline | HCID 78278 | — |
| Reactant | 2-Fluoro-5-methylaniline | HCID 262970 | — |
| Reactant | 7-Fluoro-2-iodobenzo[d]thiazole | HCID 67521180 | — |
| Product | 2-Iodo-5-methylbenzo[d]thiazole | HCID 67521101 | — |
Reaction Steps
The title compound was prepared following the route for 7-fluoro-2-iodo-1,3-benzothiazole from 2,3-difluoroaniline, starting from 2-fluoro-5-methylaniline and conducting the first step at 180° C. for 48 h in a sealed tube.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178668B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-ad3a3a295ccf4c3587269cda83d26021 |
| Source note | uspto-grants-2012_05 |