7-Bromo-2-methylsulfanyl-1,3-benzothiazole → HCID 67520750, compound

HRID 1926424Notes

Reaction equation

HRID 1926424 reaction equation
Br[C:2]1[C:10]2[S:9][C:8]([S:11][CH3:12])=[N:7][C:6]=2[CH:5]=[CH:4][CH:3]=1.[C:13]([Cu])#[N:14]>CN(C=O)C>[CH3:12][S:11][C:8]1[S:9][C:10]2[C:2]([C:13]#[N:14])=[CH:3][CH:4]=[CH:5][C:6]=2[N:7]=1

Participants

4

Reactant 2

HCID 667606187-Bromo-2-methylsulfanyl-1,3-benzothiazoleHCID 178418546HCID 178418546, compound

Product 1

HCID 67520750HCID 67520750, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The title compound was prepared from 7-bromo-2-methylsulfanyl-1,3-benzothiazole by heating with CuCN (1.0 eq.) in DMF at 160° C. for 12 h.

Sources & evidence

ORD record
ord-54d08228fd0f4033ae813c35559a1d64
Source dataset
uspto-grants-2012_05
Patent number
US08178668B2

Reaction notes

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