HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67520443, compound → HCID 67521430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67520443 | HCID 67520443 | — |
| Reactant | HCID 67520656 | HCID 67520656 | — |
| Product | HCID 67521430 | HCID 67521430 | — |
Reaction Steps
Following the procedure for 3-(7-fluoro-4-trifluoromethylbenzothiazol-2-yl)-5-(1-piperidin-4-yl-1H-pyrazol-4-yl)-pyridin-2-ylamine, using 2-iodo-5,6,7,8-tetrahydro-4H-cycloheptathiazole and conducting the Suzuki coupling at 55° C. for 3 h, the title compound was obtained as a yellow solid. MS (ES+): m/z=395.19 [MH+]. HPLC: tR=2.21 min (ZQ3, polar—5 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178668B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-b26ca5833465494ba842ac7205ed9873 |
| Source note | uspto-grants-2012_05 |