HuagongsheHuagongshe Chemistry Print Report · For research reference only
82420-39-1 → HCID 59627195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 82420-39-1 | HCID 12761383 | — |
| Reactant | HCID 59627070 | HCID 59627070 | — |
| Reactant | HCID 131729729 | HCID 131729729 | — |
| Product | HCID 59627195 | HCID 59627195 | — |
Reaction Steps
2-Amino-3-(5-chloro-3-methyl-2-nitrophenyl)propanoic acid, hydrochloride salt (40) Following the procedure for the preparation of 2-amino-3-(4-bromo-2-nitrophenyl)propanoic acid, hydrochloride salt (25) in Example 5, diethyl acetamido(5-chloro-3-methyl-2-nitrobenzyl)malonate (39) was converted to the title product, which was obtained as a solid (assumed quantitative); LCMS m/z 259.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183238B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-5db988dd345d4d80bf8b1774ad127bc9 |
| Source note | uspto-grants-2012_05 |