反应详情

温度

70 °C

A solution of 2 g (13.49 mmol) of 4-tert-butyltoluene is mixed with 5.65 g (13.49 mmol) of benzyltrimethylammonium tetrachloroiodate and stirred at 70° C. for 24 hours. After cooling, the precipitate is filtered off with suction and the filtrate is concentrated. The resulting residue is purified over silica gel (mobile phase: cyclohexane). 1.53 g (8.4 mmol) of the title compound are obtained.

1. temperatureAfter cooling
2. filtrationthe precipitate is filtered off with suction
3. concentrationthe filtrate is concentrated
4. customThe resulting residue is purified over silica gel (mobile phase: cyclohexane)