HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86641804, compound → HCID 86641803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86641804 | HCID 86641804 | — |
| Solvent | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Product | HCID 86641803 | HCID 86641803 | — |
Reaction Steps
This compound is isolated from a diastereomeric mixture of 2-hydroxy-N,N-dimethyl-3-{2-[(R)-1-(5-methyl-tetrahydrofuran-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzamide (Example 1) using reverse phase mass directed HPLC Column HICHROM HIRPB: 250×20 mm, 10 μm, eluent: 5-20% MeCN/H2O-0.1% diethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183281B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-7c138e81971e4efd96ac1a1e434d4102 |
| Source note | uspto-grants-2012_05 |