HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylfurfural → HCID 178425542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylfurfural | HCID 12097 | — |
| Reactant | (R)-beta-aminophenethyl alcohol | HCID 2724025 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178425542 | HCID 178425542 | — |
Reaction Steps
73.8 ml of 5-Methylfuran-2-carbaldehyde are added to 100 g of (R)-2-amino-2-phenyl-ethanol dissolved in 800 ml of THF. A reaction mixture obtained is heated at reflux for 5.5 hours and after cooling to rt solvent is evaporate. The title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183281B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-c9afce74120a4f29aabff2585a9f0ba3 |
| Source note | uspto-grants-2012_05 |