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HRID1927821

反应详情

EQUATION

反应方程式

HRID 1927821 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：Cc1cc(-c2ccc(Cl)cc2)nc(=O)[nH]1
HCID57468613

4-(4-Chlorophenyl)-6-methyl-2(1H)-pyrimidinone

C11H9ClN2O

PRODUCTS

生成物

1
结构：Cc1cc(-c2ccc(Cl)cc2)nc(Cl)n1
HCID20225570

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-chloro-phenyl)-6-methyl-1H-pyrimidin-2-one (11.0 g, 50.0 mmol) and phosphoryl chloride (20 mL) according to step 3 of the general procedure I. Obtained as an off-white solid (6.8 g, 57%). MS (ISP) 239.0 [(M+H)+]; mp 116-117° C.