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HRID1927852

反应详情

EQUATION

反应方程式

HRID 1927852 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：O=c1nc(-c2ccc(C(F)(F)F)cc2F)cc(C(F)(F)F)[nH]1
HCID57468689

未命名化合物

PRODUCTS

生成物

1
结构：Fc1cc(C(F)(F)F)ccc1-c1cc(C(F)(F)F)nc(Cl)n1
HCID57468688

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(2-fluoro-4-trifluoromethyl-phenyl)-6-trifluoromethyl-1H-pyrimidin-2-one (9.84 g, 0.03 mol) and phosphoroxychloride (50 ml) according to the general procedure I. Obtained as a light yellow solid (9.99 g, 96%). MS (ISN) 341.2 [(M−H)−]; mp 47° C.