HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 60209325, compound → HCID 60209336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 60209325 | HCID 60209325 | — |
| Reactant | HCID 178418934 | HCID 178418934 | — |
| Product | HCID 60209336 | HCID 60209336 | — |
Reaction Steps
The title compound was prepared from 2-chloro-4-[3-(2,2,2-trifluoro-ethoxy)-4-trifluoromethyl-phenyl]-6-trifluoromethyl-pyrimidine (example A.39) (0.85 g, 2.0 mmol) and commercially available 4-bromo-imidazole (0.44 g, 3.0 mmol) according to the general procedure IVa. Obtained as a light yellow solid (0.83 g, 78%). MS (ISP) 535.0 [(M+H)+]; mp 159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-1863ef9d64904903b8196c92a001f702 |
| Source note | uspto-grants-2012_05 |