HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57468674, compound → HCID 57468798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57468674 | HCID 57468674 | — |
| Reactant | HCID 178506559 | HCID 178506559 | — |
| Product | HCID 57468798 | HCID 57468798 | — |
Reaction Steps
The title compound was prepared from 2-chloro-4-(3,4-dichloro-phenyl)-6-methyl-pyridine (example A.51) (3.5 g, 12.8 mmol) and commercially available 4-iodo-imidazole (2.99 g, 15.4 mmol) according to the general procedure IVa. Obtained as a light grey solid (0.90 g, 16%). MS (ISP) 430.0 [(M+H)+], 432.1 [(M+2+H)+] and 434.0 [(M+4+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-259e4c3a31ad46959ab4e60a4c26303e |
| Source note | uspto-grants-2012_05 |