HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Sulfamoylbenzoic acid → HCID 57468846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Sulfamoylbenzoic acid | HCID 229352 | — |
| Reactant | HCID 178513397 | HCID 178513397 | — |
| Product | HCID 57468846 | HCID 57468846 | — |
Reaction Steps
The title compound was prepared from 4-(4-chloro-phenyl)-N-hydroxy-6-trifluoromethyl-pyrimidine-2-carboxamidine (example C.1) (0.16 g, 0.5 mmol) and commercially available 3-sulfamoyl-benzoic acid (0.1 g, 0.5 mmol) according to the general procedure VI. Obtained as a white solid (0.1 g, 43%). MS (ISP) 482.1 [(M+H)+]; mp 273° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-bf7193f8117d4b369b29e8692dbda490 |
| Source note | uspto-grants-2012_05 |