HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl chloroformate → HCID 25175256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl chloroformate | HCID 18052 | — |
| Reactant | 5-((2-(piperidin-4-yl)-2H-1,2,3-triazol-4-yl)methoxy)-2-(1H-tetrazol-1-yl)pyridine hydrochloride | HCID 68746624 | — |
| Product | HCID 25175256 | HCID 25175256 | — |
Reaction Steps
The title compound was synthesized from Intermediate 15 and allyl chloroformate in a manner similar to that described in Journal of Medicinal Chemistry 1998, 41, 4983-4994. 1H NMR (CDCl3): δ 9.46 (1H, s), 8.28 (1H, m), 8.04 (1H, m), 7.73 (1H, s), 7.61 (1H, m), 5.95 (1H, m), 5.40-5.20 (4H, m), 4.64 (3H, m), 4.24 (2H, m), 3.10 (2H, m), 2.16 (4H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183381B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-155e6fcd58bd4ffd8c141cddd730e6e2 |
| Source note | uspto-grants-2012_05 |