Hydroxyamine hydrochloride → HCID 86634185, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the above described 4-(2-methoxy-ethoxy)-benzofuran-3-one (1.9 g, 9 mmol), sodium acetate (1.5 g, 19 mmol) and hydroxylamine hydrochloride (1.3 g, 19 mmol) in ethanol (15 mL) was refluxed for 4 h. Cooled to 23° C., filtered the precipitate off, washed with water and ethanol and dried in high vacuum to give the title compound as a white solid (1.45 g, 71%); MS: m/e=224.1 (M+H−).

Provenance & Evidence