HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methylpiperazin-1-yl)acetic acid → HCID 68913013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methylpiperazin-1-yl)acetic acid | HCID 2762732 | — |
| Reactant | HCID 68631849 | HCID 68631849 | — |
| Product | HCID 68913013 | HCID 68913013 | — |
Reaction Steps
The title compound was prepared from rac-N2-(4-methoxy-2,3-dihydro-benzofuran-3-yl)-quinoline-2,6-diamine (Example 173) (150 mg, 0.59 mmol) and commercially available (4-methyl-piperazin-1-yl)-acetic acid (77 mg, 0.68 mmol) in accordance with the general method 14 described in example 119 and was obtained as an off-white solid (210 mg, 96%); MS: m/e=448.3 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183380B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-e27e9e7947d241f1bb4c28d96b71a57f |
| Source note | uspto-grants-2012_05 |