1,1-Dimethylhydrazine → HCID 18606553, compound

HRID 1929000Notes

Reaction equation

HRID 1929000 reaction equation
[CH3:1][N:2]([CH3:4])[NH2:3].[CH2:5]([N:12]1[CH2:17][CH2:16][C:15](=O)[CH:14]([CH3:19])[CH2:13]1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>C(O)C>[CH2:5]([N:12]1[CH2:17][CH2:16]/[C:15](=[N:3]\[N:2]([CH3:4])[CH3:1])/[CH:14]([CH3:19])[CH2:13]1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 2

HCID 59761,1-DimethylhydrazineHCID 5609651-Benzyl-3-methyl-4-piperidone

Product 1

HCID 18606553HCID 18606553, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

N,N-dimethylhydrazine (3 ml, 39.3 mmol) and 1-benzyl-3-methyl-piperidin-4-one (4 g, 19.7 mmol) are dissolved in 50 ml of ethanol and refluxed for 18 hours. The reaction mixture is evaporated under reduced pressure and dried at high vacuum.

Workup

  1. temperaturerefluxed for 18 hours
  2. customThe reaction mixture is evaporated under reduced pressure
  3. customdried at high vacuum

Sources & evidence

ORD record
ord-eed35e12d54e421aa716f2d7d114333c
Source dataset
uspto-grants-2012_05
Patent number
US08183366B2

Reaction notes

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