HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzyl-3,5-dimethylpiperidin-4-one → 1-Benzyl-3,5-dimethylpiperidin-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzyl-3,5-dimethylpiperidin-4-one | HCID 22278920 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Benzyl-3,5-dimethylpiperidin-4-ol | HCID 23003666 | — |
Reaction Steps
Sodiumboronhydride (121 mg, 3.2 mmol) is added to a solution of 44 (1.4 g, 6.4 mmol) in 15 ml of methanol and the mixture is stirred at room temperature for 30 min. The mixture is evaporated, and the residue is dissolved in ethyl acetate and washed with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183366B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-256fbf3064dd4b13b57874ec3c1fbcf9 |
| Source note | uspto-grants-2012_05 |