HRID1929066

反应详情

EQUATION

反应方程式

HRID 1929066 的结构方程式

PROCEDURE

实验过程

This compound is synthesized analogously to (85) from 3,3-dimethyl-butan-1-ol. Yield: 1.1 g (100%). MS (ESI): 260 [M−H]−, 1H-NMR (DMSO-d6): δ (ppm) 12.8 (s, 1H), 11.65 (s, 1H), 7.12 (dd, 1H), 6.98 (s, 1H), 6.95 (d, 1H), 6.52 (d, 1H), 4.13 (t, 2H), 1.75 (t, 2H), 1.0 (s, 9H).