HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Thiocarbonyldiimidazole → HCID 59550995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Reactant | HCID 59551030 | HCID 59551030 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59550995 | HCID 59550995 | — |
Reaction Steps
To a solution of 1-isopropyl-7-methoxy-1H-indol-4-ylamine (U) (1 eq) in dichloromethane was added 1,1′-thiocarbonyldiimidazole (1.2 eq). The reaction was stirred for 2 hrs at room temperature then evaporated to dryness. Further purification by column chromatography produced the pure desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188075B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-65452fc5cba84c1fa7d1f4b63eb2f752 |
| Source note | uspto-grants-2012_05 |