HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,4-Trichloro-3-[1-(2-fluoro-4-nitrophenoxy)ethyl]benzene → 3-Fluoro-4-[1-(2,3,6-trichlorophenyl)ethoxy]aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,4-Trichloro-3-[1-(2-fluoro-4-nitrophenoxy)ethyl]benzene | HCID 68511440 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Fluoro-4-[1-(2,3,6-trichlorophenyl)ethoxy]aniline | HCID 68512300 | — |
Reaction Steps
3-Fluoro-4-[1-(2,3,6-trichlorophenyl)ethoxy]aniline was prepared according to the method described in Example 20e but from 0.093 g of platinum oxide and 1.5 g of 1,2,4-trichloro-3-[1-(2-fluoro-4-nitrophenoxy)ethyl]benzene in 100 cm3 of methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188078B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-3214bedd94774c1ebe5e02e2d4171ed2 |
| Source note | uspto-grants-2012_05 |