HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67389700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57474951 | HCID 57474951 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Triethylsilane | HCID 12052 | — |
| Product | HCID 67389700 | HCID 67389700 | — |
Reaction Steps
A solution of EXAMPLE 22C (0.85 g, 1.4 mmol) in dichloromethane (10 mL), trifluoroacetic acid (10 mL) and triethylsilane (1 mL) was stirred for 24 hours. The mixture was concentrated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188077B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-a970b5c3603b436bbb234b4c1935c257 |
| Source note | uspto-grants-2012_05 |