HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanoic acid, 2-bromo-2-methyl-, ethyl ester → HCID 10848710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanoic acid, 2-bromo-2-methyl-, ethyl ester | HCID 11745 | — |
| Reactant | 2-Amino-4-chloro-5-nitrophenol | HCID 3894848 | — |
| Product | HCID 10848710 | HCID 10848710 | — |
Reaction Steps
2-amino-4-chloro-5-nitrophenol (10.0 g) and ethyl α-bromoisobutyrate (7.4 mL) were treated in the same manner as described in Reference Example 1(1) to give 6-chloro-2,2-dimethyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one (6.82 g) as a pale brown powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188073B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-b479097946bb49d9bafea2ddfbc30b79 |
| Source note | uspto-grants-2012_05 |