HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromobutane → HCID 66931655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromobutane | HCID 6554 | — |
| Reactant | 5-Chloro-2-picolinic acid | HCID 2762872 | — |
| Reactant | HCID 66931452 | HCID 66931452 | — |
| Product | HCID 66931655 | HCID 66931655 | — |
Reaction Steps
The (RS)-3-sec-butyl-5-chloro-pyridine-2-carboxylic acid was prepared in analogy to the preparation of 5-chloro-3-ethyl-pyridine-2-carboxylic acid by treatment of 5-chloropyridine-2-carboxylic acid with 2-bromo-butane. The (RS)-3-sec-butyl-5-chloro-pyridine-2-carboxylic acid was obtained as a white solid (yield: 6% of theory). Mass (calculated) C10H12ClNO2 [213.66]; (found) [M+H]+=213, [M+2-H]+=215.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188079B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-1f0987db645c4d76b6c5e318880db74f |
| Source note | uspto-grants-2012_05 |