HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68973103, compound → HCID 68972653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68973103 | HCID 68973103 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68972653 | HCID 68972653 | — |
Reaction Steps
A mixture of P5 (0.12 mmol) and Pd/C (10%, 22 mg) in MeOH (0.2 M) was stirred under H2 atmosphere overnight. The catalyst was filtered off and the solvent removed under reduced pressure to provide a crude oil used as such in the next step. MS (ES) C10H19N5 required: 209. found: 210 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188084B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-8834e859aae441f7abe7f97acbd1c0cf |
| Source note | uspto-grants-2012_05 |