Ammonia → HCID 24205344, compound

Participants

Reaction Steps

General procedure e from 17 (100%); white powder; mp 147-149° C.; 1H NMR (400.13 MHz) δ 8.11 (d, J=4 Hz, 1H), 7.84 (d, J=2 Hz, 1H), 7.75 (s, 1H), 7.42 (s, 1H), 7.40 (d, J=4 Hz, 2H), 7.30 (t, J=4 Hz, 2H), 7.27 (m, 1H), 7.23 (dd, J=4 Hz, 2 Hz, 1H), 7.14 (s, 1H), 6.01 (s, 2H), 5.16 (s, 2H), 4.30 (s, 2H), 3.24 (m, 1H), 2.48 (m, 2H), 2.0 (m, 2H), 1.68 (m, 2H); MS (DCI/NH3) m/e: 456 (M+H)+. Anal. (C28H25O5N.1.0H2O) C, H, N.

Provenance & Evidence