Ammonia → HCID 86625134, compound

Participants

Reaction Steps

General procedure g from 16 (92%); white powder; mp 230-231° C.; 1H NMR (400.13 MHz) δ 7.73 (d, J=4 Hz, 1H), 7.67 (s, 1H), 7.50 (d, J=2 Hz, 1H), 7.35 (s, 1H), 7.21 (dd, J=4 Hz, 2 Hz, 1H), 7.06 (m, 1H), 6.01 (s, 2H), 4.67 (t, J=7 Hz, 1H), 3.22 (m, 2H), 2.38 (m, 2H), 2.18 (m, 2H), 1.86 (m, 2H); MS (DCI/NH3) m/e: 380 (M+H)+.

Provenance & Evidence