Ammonia → HCID 86625135, compound

Participants

Reaction Steps

General procedure g from 18 (95%); white powder; mp 205-206° C.; 1H NMR (400.13 MHz) δ 8.07 (d, J=4 Hz, 1H), 7.82 (s, 1H), 7.80 (d, J=2 Hz, 1H), 7.42 (s, 1H), 7.21 (dd, J=4 Hz, 2 Hz, 1H), 7.10 (s, 1H), 6.04 (s, 2H), 4.09 (s, 2H), 3.16 (m, 1H), 2.38 (m, 2H), 2.23 (m, 2H), 1.95 (m, 2H); MS (DCI/NH3) m/e: 366 (M+H)+.

Provenance & Evidence