Ammonia → HCID 86625137, compound

Participants

Reaction Steps

General procedure f from 35 (92%); yellow oil; 1H NMR (400.13 MHz) δ 7.88 (d, J=4 Hz, 1H), 7.76 (s, 1H), 7.71 (d, J=2 Hz, 1H), 7.44 (s, 1H), 7.13 (dd, J=4 Hz, 2 Hz, 1H), 7.05 (s, 1H), 5.99 (s, 2H), 3.94 (s, 9H), 3.80 (s, 2H), 3.73 (t, J=6 Hz, 2H), 2.75 (m, 2H), 1.50 (m, 4H), 1.28 (m, 4H); MS (DCI/NH3) m/e: 398 (M+H)+.

Provenance & Evidence