Ammonia → HCID 69277495, compound

Participants

Reaction Steps

General procedure d from 39 (90%); brown syrup; 1H NMR (400.13 MHz) δ 7.61 (s, 1H), 7.24 (d, J=4 Hz, 2H), 7.01 (s, 1H), 6.77 (d, J=4 Hz, 2H), 6.64 (s, 1H), 4.36 (d, J=7 Hz, 2H), 3.89 (s, 3H), 3.72 (t, J=7 Hz, 1H), 3.69 (s, 3H), 3.42 (s, 3H), 3.24 (m, 2H), 2.18 (m, 2H), 1.84 (m, 2H); MS (DCI/NH3) m/e: 429 (M+H)+.

Provenance & Evidence