Ammonia → HCID 69276492, compound

Participants

Reaction Steps

General procedure f from 40 (90%); dark oil; 1H NMR (400.13 MHz) δ 7.59 (s, 1H), 7.23 (d, J=4 Hz, 2H), 7.00 (s, 1H), 6.71 (d, J=4 Hz, 2H), 6.23 (s, 1H), 4.17 (d, J=7 Hz, 2H), 3.89 (s, 3H), 3.78 (d, J=7 Hz, 2H), 3.69 (s, 3H), 3.58 (m, 1H), 3.41 (s, 3H), 3.16 (m, 2H), 1.91 (m, 2H), 1.80 (m, 2H); MS (DCI/NH3) m/e: 415 (M+H)+.

Provenance & Evidence