Ammonia → HCID 16749052, compound

Participants

Reaction Steps

N-(2,3-Methylenedioxy-6-methoxy-phenanthr-9-ylmethyl)-6-aminohexanol hydrochloride (22b) White powder; mp 187-188° C.; 1H NMR (400.13 MHz) δ δ 8.14 (d, J=4 Hz, 1H), 7.82 (s, 1H), 7.76 (d, J=2 Hz, 1H), 7.50 (s, 1H), 7.18 (dd, J=4 Hz, 2 Hz, 1H), 7.13 (s, 1H), 6.08 (s, 2H), 4.67 (s, 2H), 3.98 (s, 3H), 3.60 (t, J=6 Hz, 2H), 3.44 (m, 2H), 1.66 (m, 2H), 1.59 (m, 2H), 1.40 (m, 2H), 1.33 (m, 2H); MS (DCI/NH3) m/e: 382 (M+H)+. Anal. (C23H27O4N.1.0HCl.1.5H2O) C, H, N.

Provenance & Evidence