HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malonic Acid → HCID 53395407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | 2,4-Dimethylbenzaldehyde | HCID 61814 | — |
| Product | HCID 53395407 | HCID 53395407 | — |
Reaction Steps
According to the previously described general procedure (GP1), Knoevenagel condensation (75° C.; 3h30) between 2,4-dimethyl-benzaldehyde (10.000 g; 74.528 mmol) and malonic acid (14.735 g; 141.607 mmol) gave the product 3-(2,4-dimethyl-phenyl)-acrylic acid as a colorless solid (9.720 g; 74%). LC-MS: tR=0.86 min; [M+H]+: no ionisation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188082B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-3a15e183d053496eba6c1e98fa8c4e6b |
| Source note | uspto-grants-2012_05 |