HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Iodo-3-isopropyl-[1,2,4]triazolo[4,3-b]pyridazine → HCID 57929864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Iodo-3-isopropyl-[1,2,4]triazolo[4,3-b]pyridazine | HCID 57929893 | — |
| Reactant | HCID 57929922 | HCID 57929922 | — |
| Product | HCID 57929864 | HCID 57929864 | 22.1% |
Reaction Steps
6-Iodo-3-isopropyl-[1,2,4]triazolo[4,3-b]pyridazine (0.400 g, 1.25 mmol, Preparation #H.1) and 3-(2,4-difluorophenyl)-4-iodo-5-methylisoxazole (0.360 g, 1.25 mmol) were coupled using General Procedure I.1 to provide the title compound (0.098 g, 22%): LC/MS (Table 1, Method g) Rt=2.16 min; MS m/z: 356.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188083B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-123cb68a344942b7b6597c8772d884da |
| Source note | uspto-grants-2012_05 |