HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Fluoro-7-bromoisoquinoline → 7-Bromo-6-fluoro-isoquinoline 2-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Fluoro-7-bromoisoquinoline | HCID 53402964 | — |
| Reactant | 7-Chloro-6-fluoro-isoquinoline 2-oxide | HCID 59818254 | — |
| Product | 7-Bromo-6-fluoro-isoquinoline 2-oxide | HCID 59818251 | — |
Reaction Steps
Starting from 7-bromo-6-fluoro-isoquinoline (15), the title compound was prepared following the method described for 7-chloro-6-fluoro-isoquinoline 2-oxide (5). Rt=0.93 min (Method C). Detected mass: 242.2/244.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188117B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-f30c45a39b184f739854cbd83f42d47a |
| Source note | uspto-grants-2012_05 |