HRID1930228

反应详情

EQUATION

反应方程式

HRID 1930228 的结构方程式

PROCEDURE

实验过程

4-[7-Ethyl-2-(4-methoxy-benzyl)-1-oxo-1,2-dihydro-isoquinolin-6-yloxy]-piperidine-1-carboxylic acid tert-butyl ester (319) is deprotected following the method described for 7-bromo-6-(piperidin-4-yloxy)-2H-isoquinolin-1-one (17). Final purification by preparative HPLC delivers the title compound as trifluoroacetate. Rt=0.92 min (Method A). Detected mass: 273.2 (M+H+).

WORKUP

后处理

  1. customFinal purification by preparative HPLC