HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-oxopiperidine-1-carboxylate → HCID 59333721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Reactant | 2-(2-Fluorophenyl)acetyl chloride | HCID 14004011 | — |
| Product | HCID 59333721 | HCID 59333721 | 52% |
Reaction Steps
tert-Butyl 3-(2-(2-fluorophenyl)acetyl)-4-oxopiperidine-1-carboxylate (295 mg, 52%) was synthesised from tert-butyl 4-oxopiperidine-1-carboxylate and 2-(2-fluorophenyl)acetyl chloride according to the general procedure for the preparation of diketones. MS (ES−) m/z 334.1(M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-a0bf223f0c2a49ff98a7a1cf0230d939 |
| Source note | uspto-grants-2012_05 |