HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-oxopiperidine-1-carboxylate → Tert-butyl 3-(2-cyclopentylacetyl)-4-oxopiperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Reactant | Cyclopentylacetyl chloride | HCID 3485182 | — |
| Product | Tert-butyl 3-(2-cyclopentylacetyl)-4-oxopiperidine-1-carboxylate | HCID 59333704 | 59% |
Reaction Steps
tert-Butyl 3-(2-cyclopentylacetyl)-4-oxopiperidine-1-carboxylate (311 mg, 59%) was synthesised from tert-butyl 4-oxopiperidine-1-carboxylate and 2-cyclopentylacetyl chloride according to the general procedure for the preparation of diketones. MS (ES−) m/z 308.1 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-b1880c95c18f4d8dbce6b41865567530 |
| Source note | uspto-grants-2012_05 |