HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 46199113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 59333774 | HCID 59333774 | — |
| Product | HCID 46199113 | HCID 46199113 | 10.6% |
Reaction Steps
1-(2-(4-(2-Methyl-1H-imidazol-1-yl)phenylamino)-4-(4-methylbenzyl)-7,8-dihydropyrido[4,3-d]pyrimidin-6(5H)-yl)ethanone (11.3 mg, 10.6%) was synthesised from N-(4-(2-methyl-1H-imidazol-1-yl)phenyl)-4-(4-methylbenzyl)-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidin-2-amine (Example 50a) and acetic anhydride according to the general procedure for N-acetylation. MS (ES+) m/z 453.2 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-f518407babb8449091535d55009514f0 |
| Source note | uspto-grants-2012_05 |