Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59333740 | HCID 59333740 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59333775 | HCID 59333775 | — |
Reaction Steps
(S)-tert-Butyl 2-(4-(oxazol-5-yl)phenylamino)-4-((tetrahydrofuran-2-yl)methylamino)-7,8-dihydropyrido[4,3-d]pyrimidine-6(5H)-carboxylate was dissolved in methanol (3 mL). Hydrochloric acid was added and the reaction mixture was stirred at 75° C. for 1 h. The solvent was evaporated under reduced pressure and the crude was used as such in the next step. MS (ES+) m/z 393.2 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08188101B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-94ac3f8298524795ba7c89948d7d2e6e |
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| Source note | uspto-grants-2012_05 |
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