HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethoxalyl chloride → HCID 59333783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethoxalyl chloride | HCID 20884 | — |
| Reactant | Tetrahydro-4H-pyran-4-one | HCID 121599 | — |
| Product | HCID 59333783 | HCID 59333783 | 19% |
Reaction Steps
Ethyl 2-oxo-2-(4-oxotetrahydro-2H-pyran-3-yl)acetate (272 mg, 19%) was synthesised from tetrahydro-4H-pyran-4-one (1 ml, 10.83 mmol) and ethyl 2-chloro-2-oxoacetate (0.808 ml, 7.22 mmol) by the general procedure for the preparation of diketones. MS (ES−) m/z 199.1 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-65f52fdf3681472e8fb31869a3fef975 |
| Source note | uspto-grants-2012_05 |