HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydro-4H-pyran-4-one → 3-(2-(Cyclopentyloxy)acetyl)dihydro-2H-pyran-4(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydro-4H-pyran-4-one | HCID 121599 | — |
| Reactant | 2-(Cyclopentyloxy)acetyl chloride | HCID 86641917 | — |
| Product | 3-(2-(Cyclopentyloxy)acetyl)dihydro-2H-pyran-4(3H)-one | HCID 59333715 | 37.5% |
Reaction Steps
3-(2-(cyclopentyloxy)acetyl)dihydro-2H-pyran-4(3H)-one (280 mg, 21.5%) was synthesised from dihydro-2H-pyran-4(3H)-one (0.462 ml, 5.00 mmol) and (2-(cyclopentyloxy)acetyl chloride (3.3 mmol) by the general procedure for the preparation of diketones.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-a05ef98cc5014ca9b575f0b3ef12da94 |
| Source note | uspto-grants-2012_05 |