HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 59333797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | Tetrahydrothiopyran-4-one | HCID 66173 | — |
| Product | HCID 59333797 | HCID 59333797 | 83% |
Reaction Steps
3-(2-Phenylacetyl)dihydro-2H-thiopyran-4(3H)-one (291 mg, 83%) was synthesised from 2-phenylacetyl chloride and dihydro-2H-thiopyran-4(3H)-one according to the general procedure for the preparation of diketones. MS (ES−) m/z 233 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-2c1c1d34a831448aa3688a8620b8f1df |
| Source note | uspto-grants-2012_05 |