HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannane, tributyl(1-ethoxyethenyl)- → 1-(6-Trifluoromethyl-2,3-dihydro-1H-isoindol-5-yl)-ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannane, tributyl(1-ethoxyethenyl)- | HCID 619414 | — |
| Reactant | HCID 57753490 | HCID 57753490 | — |
| Product | 1-(6-Trifluoromethyl-2,3-dihydro-1H-isoindol-5-yl)-ethanone | HCID 57753281 | — |
Reaction Steps
Prepared in analogy to Example A47 from 5-iodo-6-trifluoromethyl-1,3-dihydro-isoindole-2-carboxylic acid tert-butyl ester (Example A35(d)) and 1-ethoxyvinyltributylstannane. White solid. MS (m/e): 230.3 ([M+H]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188139B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-6da8c10a1ed04f42b34439988812fc48 |
| Source note | uspto-grants-2012_05 |