反应详情

温度

200 °C

A mixture of 144 mmol 4-fluorophthalic anhydride and 1.16 mol formamide was heated at 200° C. for 2 h. The reaction mixture was poured onto ice-water and the resulting crystals collected by filtration and dried in vacuo to afford the title compound as a yellow solid (100% yield). MS (m/e): 164.4 ([M−H]−, 100%).

1. additionThe reaction mixture was poured onto ice-water
2. filtrationthe resulting crystals collected by filtration
3. customdried in vacuo