HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15289013, compound → 2-Acetylamino-7-benzoylamino-4-octenedioic acid dimethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15289013 | HCID 15289013 | — |
| Reactant | HCID 66776746 | HCID 66776746 | — |
| Product | 2-Acetylamino-7-benzoylamino-4-octenedioic acid dimethyl ester | HCID 66775906 | — |
Reaction Steps
2-Acetylamino-7-benzoylamino-4-octenedioic acid dimethyl ester 142 was synthesised using standard solution-phase metathesis conditions (refer to section 7.5) from 6-acetoxy-2-benzoylamino-4-hexenoic acid methyl ester 141 and methyl-2-acetylamino-4-pentenoate 121a. The desired compound was obtained as a brown oil, and purified via column chromatography (SiO2; EtOAc:Hexane; 2:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188217B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-d8369f5234494e7ab8918a91b1091ba1 |
| Source note | uspto-grants-2012_05 |